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1 article(s) from Hayashi, Hironobu

Direct borylation of terrylene and quaterrylene

Haruka Kano,
Keiji Uehara,
Kyohei Matsuo,
Hironobu Hayashi,
Hiroko Yamada and
Naoki Aratani

Beilstein J. Org. Chem. 2020, 16, 621–627, doi:10.3762/bjoc.16.58

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Figure 1: Chemical structures of a) oligorylene-bisimides, b) oligorylenes, c) bay-bridging oligorylenes, d) ...

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Scheme 1: Synthesis of 2,5,10,13-tetrakis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)terrylene (TB4): (a) (B...

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Figure 2: (Top) Single crystal X-ray structure of TB4. The thermal ellipsoids are scaled at 50% probability. ...

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Figure 3: UV–vis absorption and fluorescence spectra of terrylene (black) and TB4 (red) in toluene. λ_ex = 489...

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Figure 4: MO diagrams of terrylene and TB4 based on calculations at the B3LYP/6-31G(d).

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Scheme 2: Synthesis of 2,5,12,15-tetrakis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)quaterrylene (QB4): (a)...

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Figure 5: UV–vis absorption spectrum of QB4 in toluene.

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Figure 6: MO diagrams of terrylene and QB4 based on calculations at the B3LYP/6-31G(d).

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Scheme 3: Suzuki–Miyaura cross-coupling reaction of TB4 with 2-bromomesitylene. (a) 2-bromomesitylene (8 equi...

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Published 06 Apr 2020

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